CN100574745C - Cosmetic composition for scrubbing - Google Patents
Cosmetic composition for scrubbing Download PDFInfo
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- CN100574745C CN100574745C CN200580005586A CN200580005586A CN100574745C CN 100574745 C CN100574745 C CN 100574745C CN 200580005586 A CN200580005586 A CN 200580005586A CN 200580005586 A CN200580005586 A CN 200580005586A CN 100574745 C CN100574745 C CN 100574745C
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- scrubbing
- cosmetic composition
- bracken
- spore
- composition
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
- A61K8/022—Powders; Compacted Powders
- A61K8/0225—Granulated powders
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9741—Pteridophyta [ferns]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
Abstract
A kind of cosmetic composition for scrubbing is provided, and it contains, and to increase skin blood by friction on skin mobile and remove cuticular scrub particle, and wherein, this scrub particle is a bracken spore.When friction is during this cosmetic composition for scrubbing on skin, a plurality of hydranths that form on the bracken spore surface are broken, so this cosmetic composition for scrubbing chafe and have good use feeling and even and excellent scrub effect not.
Description
Technical field
The present invention relates to a kind of cosmetic composition for scrubbing.
Background technology
When friction on skin during cosmetic composition for scrubbing, contained scrub particle chafe in the compositions, so skin blood flows and increases and skin elasticity improves, aged horny layer also is removed, and therefore makes skin Lightening.
In general, through for example dried Semen Armeniacae Amarum of natural component of mechanical activation comminution, Semen Persicae, Semen Juglandis etc., perhaps particle diameter is that the spherical polyethylene powder of 200-500 micron is as the scrub particle of cleaning in the make-up composition.In addition, by particle diameter being about 50 microns synthetic polymer particle polyethylene, urethane (urethane) or the nylon size that the obtains bonded to each other agglomerate that is the 200-500 micron for example, can be used as scrub particle.
Yet because the scrub particle of being made by synthetic polymer is hard, they are not easy fragmentation when rubbing on skin.Therefore, the relatively poor and chafe of use feeling that contains the cosmetic composition for scrubbing meeting of the scrub particle of making by synthetic polymer.And they can not provide uniform scrub effect.In addition, the natural granule for example surface point of broken Semen Armeniacae Amarum is hard, rough, therefore may scratch skin.
Summary of the invention
The invention provides a kind of not chafe and have good use feeling and the cosmetic composition for scrubbing of even and excellent scrub effect.
According to an aspect of the present invention, provide a kind of cosmetic composition for scrubbing, said composition contains that to increase skin blood by friction on skin mobile and remove cuticular scrub particle, and wherein this scrub particle is bracken spore (bracken spore).
Bracken spore can add with the form of a plurality of bracken spores through binding agent pearl bonded to one another.On the surface of each pearl, can also be formed with coating.
According to an embodiment of the invention, contain bracken spore and can make following preparation: cleansing cream, gel, foam, powder (powder), body wash, scouring shampoo or massage cream as the cosmetic composition for scrubbing of scrub particle.It can be used for facial cleaning, bathing, hair washing, skin massaging etc.
Description of drawings
With reference to accompanying drawing, by describing typical embodiment in detail, of the present invention above and further feature and advantage will become more obvious, wherein:
Fig. 1 is the electron micrograph according to the cross section of employed bracken spore in the cosmetic composition for scrubbing of an embodiment of the invention;
Fig. 2 is the electron micrograph on employed bracken spore surface in the cosmetic composition for scrubbing according to an embodiment of the invention; With
Fig. 3 is to pass through the optical microscope photograph of binding agent (alginic acid) with a plurality of bracken spores pearl bracken spore that obtains bonded to each other.
The specific embodiment
Below, cosmetic composition for scrubbing is according to the embodiment of the present invention described in more detail.
Herba Fimbristylis dichotomae is a kind of pteridophyta from extensive growth in Paleozoic late period in the devonian period.It is grown in the area of warm moist.The climax leaves of Herba Fimbristylis dichotomae have at its back side for the Sporangium of tennis racket shape and in this Sporangium growth spore arranged.These spore-germinations form original foliages and usually sperm and the ovum by original foliage be grown to sophisticated Herba Fimbristylis dichotomae through sexual propagation.Collect the spore of Spora Lygodii (Lygodiumjaponicum) in autumn, at Compendium of Materia Medica [Li Shizhen (1518-1593 A.D.), Compendium of Materia Medica, 1596] put down in writing these spores in and be used for the treatment of urethritis and ureteral calculus etc., and hepatitis, fracture, syphilis and prostatitis have been had therapeutic effect.And, also have spore extract that report uses Spora Lygodii as brightening agent and the spore powder that uses Spora Lygodii as the cosmetic inorganic pigment.Yet also report does not use bracken spore as scrub particle.
The present inventor joins bracken spore in the make-up composition as scrub particle, and the health of being careful the specific modality structure of observing bracken spore and finding to contain bracken spore is cleaned not chafe and have good use feeling and even and excellent scrub effect of make-up composition.
With reference to Fig. 1 and 2, bracken spore is spherical and constant magnitude.The outer wall of bracken spore is made of polysaccharide skeleton (skeleton) and bracken spore has many fine water hydroids (polyp) on its surface.These hydranths are subjected to frictional force and break on skin.Conventional relatively scrub particle, because the morphosis of bracken spore, so it is little and more uniform scrub effect is provided to the stimulation of skin.
The bracken spore that is used for cosmetic composition for scrubbing of the present invention can obtain by the following method: collect wild pteridophyte and with they dryings, shake dried Herba Fimbristylis dichotomae then and therefrom take out spore.Under the preferable case, can screen the spore that particle diameter is the 10-200 micron.When bracken spore contains a large amount of impurity, for example, during sand, can remove these impurity by following method: the spore that will have impurity suspends in water and makes contamination precipitation, collection swims in the spore in the water, then with the dry bracken spore that obtains not have impurity of the spore of collecting.Perhaps, also can remove impurity contained in the bracken spore effectively by following method: the bracken spore that will contain impurity is suspended in the ethanol water of 50-70%, under the room temperature this suspended substance is left standstill 24 hours at least, collects bracken spore and dry.
If necessary, bracken spore can be through sterilization process and the process of removing extract.This sterilization process can use conventional method to carry out, for example ethylene oxide gas sterilization, high steam sterilization or radicidation.
The bracken spore of collecting from wild pteridophyte can self join the make-up composition as scrub particle.If necessary, a plurality of bracken spores can for example be the pearl of 0.1-10 millimeter by binding agent acquisition size bonded to one another.Therefore, can control scouring intensity.The example of binding agent comprise alginic acid or alginate, Polyethylene Glycol (PEG), polyvinyl pyrrolidone (PVP), polyvinyl alcohol (PVA), hydroxypropyl cellulose (HPC), methylcellulose (MC), hydroxy methocel (HMC), hydroxypropyl emthylcellulose (HPMC), carbopol (Carboxypolymethylene, Carbopol), carboxymethyl cellulose (CMC), gelatin, starch etc.Can be that spheroidal particle or pill (pellet) obtain these pearls with Sporulation with conventional method.Term used herein " pearl (bead) " should be explained and be meant all types of powder with pre-sizing, for example Chang Gui pearl and granule.
Use alginic acid (or alginate) a plurality of bracken spores are bonded to one another and prepare the method for pearl below by case description as binding agent.
The bracken spores of 100 grams are joined in alginic acid (or alginate) aqueous solution to stir make serosity (sludge solution).Alginic acid (or alginate) aqueous solution for example can be by being that 50-2500 and mean molecule quantity are that the natural polymer of the alginic acid of 10000-500000 and/or alginate is dissolved in room temperature water or the hot water with the concentration of 0.01-5 weight % and makes with the degree of polymerization.Preferably, the ratio that can adjust bracken spore and alginic acid aqueous solution makes the weight ratio (A: be 50 B): 50-99: 1 of bracken spore (A) and dissolved alginic acid (B) in the serosity.
Then, can so that being added in the multivalent metal cation solution, this slurry drops form pearl by the pipe that is the 0.1-10 millimeter with the extruded interior diameter excessively of the serosity that obtains.Perhaps, also can form pearl in the alcoholic solution by this serosity is sprayed or under agitation serosity slowly joined.The pearl that obtains can also be with the cationic surfactant solution-treated of C12-20 alkyl or alkylidene leptodactyline for example, bonds between these pearls between dry period preventing.
Can also form coating on the surface of each pearl of Huo Deing in the above, thus further increase these pearls in make-up composition stability and improve use feeling.This coating can form by the solution of following material or suspended substance are sprayed on the pearl: Polyethylene Glycol (PEG), polyvinyl pyrrolidone (PVP), hydroxypropyl cellulose (HPC), methylcellulose (MC), hydroxy methocel (HMC), hydroxypropyl emthylcellulose (HPMC), carbopol (Carbopol), gelatin, starch, Lac or SB (SB copolymer), but the method that forms coating is not limited to this.
These bracken spores can join in the make-up composition as scrub particle with self or with the form of pearl, make formulation example such as cleansing cream, gel, foam, powder, body wash, scouring shampoo and massage cream etc.Preferably, based on this scouring make-up composition, the concentration of bracken spore can be 0.2-20 weight %.
The present invention is described in detail below with reference to embodiment.Yet these embodiments of the present invention can improve in various manners and should understand the present invention and are not limited to embodiment described below.To those of ordinary skills, only provide these embodiments of the present invention to be described as purpose.
Preparation embodiment 1
Collect wild pteridophyte and dry, obtain dry spore by shaking this drying Herba Fimbristylis dichotomae then.Screen spore and obtain the spore that particle diameter is the 10-200 micron with 50 mesh sieves.Then, the bracken spore that obtains is suspended in water and leaves standstill make contamination precipitation.Then, collect the spore and the drying that float in the water, obtain not have the bracken spore of impurity.
Preparation embodiment 2
Collect wild pteridophyte and dry, obtain dry spore by shaking this drying Herba Fimbristylis dichotomae then.The screening spore also obtains the spore that particle diameter is the 10-200 micron.Then, the bracken spore that obtains is joined in 70% ethanol of 5 times of volumes and stir.After fine deposition 24 hours, take out the part and the drying of removing outside the fine deposition thing, obtain not have the bracken spore of impurity.
Preparation embodiment 3
Restrain being equipped with the bracken spore that obtains among the embodiment 2 with 100 joins in 4 liter of 1% sodium alginate aqueous solution (40 gram alginic acid) and stirs and obtain serosity.Then, be that 3 millimeters pipe is added in the 2%CaCl2 solution this slurry drops by this serosity being pressed through internal diameter, form the alginic acid gel beads that contains a plurality of bracken spores.Gained alginic acid gel beads has the viscoelasticity network structure.The alginic acid gel beads is removed solution by net filtration, and is dry down at 60-100 ℃ then.Therefore, obtaining diameter is the alginic acid pearl that contains bracken spore of 0.2-0.7 millimeter.Fig. 3 is the optical microscope photograph of the alginic acid pearl that contains bracken spore of acquisition among the preparation embodiment 3.
Preparation embodiment 4
100 restraints are equipped with the bracken spore of acquisition among the embodiment 2 and the polyvinyl pyrrolidone (PVP K-120) of 10 grams and the carboxymethyl celluloses of 2 grams in the mixture of second alcohol and water, mediate the formation slurry.Then, 0.5 millimeter length is extruded and cut into to the extruder of the outlet of this slurry through having 0.5 millimeter internal diameter, obtains pill shape granule.Then, the granule that obtains 60-100 ℃ dry down and pour into pelletize with the centrifugal fluidized bed spreader in, with suitable speed the Lac of 5 grams and the solution of SB (SB copolymer) in the mixture of second alcohol and water of 5 grams are injected this operation spreader to form coating on particle surface.
Preparation embodiment 5
Restraining the bracken spore that is equipped with acquisition among the embodiment 2 with 100 pours in the electronic centrifugal granulator machine.Then, when rotating the container of granulator, 10% hydroxypropyl cellulose (HPC) aqueous solution is sprayed onto in this container, with suitable speed bracken spore is injected in this granulator simultaneously.Continue pelletize up to obtaining suitable spheroidal particle.The granule that obtains is dry under 60-100 ℃, and obtaining diameter is the granule that contains bracken spore of 0.3-0.5 millimeter.Then, the granule that will contain bracken spore is poured into from bottom to top in the type fluid bed spreader and with the Lac of 10 grams and the solution of hydroxypropyl emthylcellulose (HPMC) in the mixture of second alcohol and water of 2 grams and is sprayed onto on the granule with suitable speed, to form coating on particle surface.
Experimental example 1
The eye that produces when contacting with eye mucosa in order to estimate bracken spore stimulates, and " the Acute Eye Irritation/Corrosion " that measure guide according to OECD (Organization of Economy and Cooperation Development) chemical substance carries out eye irritant test.Each eye of six New Zealand white rabbit (2-3 kilogram) is handled once with the bracken spore that obtains among the preparation embodiment 2, and with the another eye in contrast.Estimate the extent of damage of cornea, iris and conjunctiva.Carry out eye examination at eye irritant test before 24 hours, will not have the rabbit of eye irritation to be used for this test.Because the powdery bracken spore is not easy administration, therefore bracken spore is suspended in the normal saline and 0.1 milliliter the suspended substance that contains 15% bracken spore is dripped in the right eye of every rabbit.At this moment, with palpebra inferior from directing one's eyes downward pull-shaped one-tenth cup-shaped and suspension dripped to the conjunctival sac.Close one's eyes about 1 second to prevent the suspended substance loss.Under the situation of not cleaning face, all animals are left.Left eye does not give test material, in contrast.The reaction that takes place in clinical symptoms and the eye based on following ocular damage grade, is estimated in after the medicine-feeding test material 1,24,48 and 72 hour.
(ocular injury grade)
(1) horny layer: A * B * 5.......... maximum=80
(A) opacity: 0-4 (B) corneal opacity degree: 1-4
(2) iris: A * 5.............. maximum=10
(A) response value: 0-2
(3) conjunctiva: (A+B+C) * 2.... maximum=20
(A) redness: 0-3 (B) chemosis: 0-4 (C) secretions: 0-3
The eye stimulation levels is as shown in table 1 below.
Table 1
| Evaluation of estimate | Test eye stimulation levels |
| 0-5 | Non-stimulated |
| 6-15 | Slightly stimulate |
| 16-30 | Stimulation is arranged |
| 31-60 | Moderate stimulates |
| 61-80 | Serious stimulate (seriously irritation) |
| 80-110 | Severe irritation (severely irritation) |
When being basic evaluation with the ocular injury grade, the bracken spore scoring is 2.0, is equivalent to " non-stimulated ".Therefore, confirm that bracken spore is used for eye mucosa safely.Observe bracken spore and also therefore do not brought out other abnormal symptom by quick discharge of tear.After the administration 2 days, in the secretions of all six animals, do not detect bracken spore.
Embodiment 1-6 and Comparative Examples 1 and 2
Chemical compound and ratio of components that use table 2 is listed prepare cleansing cream.In embodiment 1, the powder formulation that preparation only is made up of bracken spore.
Table 2
Experimental example 2
Following 8 samples to embodiment 1-6 and Comparative Examples 1 and 2 acquisitions are estimated the cuticular effects of removing.These samples had been used for 20 ages before the NAM and women of 20-40 between year, use tintometer (Dhroma meter, CR-200, Minolta, Japan) measure the color of the upper arm inside of each experimental subject, and 8 parts of upper arm (each part wide 2 centimetres, long 2 centimetres) are continued to be coated with brown in 6 hours with 10% dihydroxy acetone (DHA).Then, each sample is coated to coloured part and, washes with water then with constant force friction 2 minutes.After washing 60 minutes, measure the color of coloured part and determine that sample applies the colour-difference of front and back.Then, in the same manner as described above, sample is coated to coloured part every day 1 time, the decolouring degree is measured in friction and washing.Measure coloured part and get back to the required time of original skin color, obtain meansigma methods and be listed in table 3.
Table 3
| Sample | The regenerated natural law of horny layer |
| Embodiment 1 | 10.5 |
| Embodiment 2 | 12.7 |
| Embodiment 3 | 12.8 |
| Embodiment 4 | 12.0 |
| Embodiment 5 | 12.2 |
| Embodiment 6 | 12.4 |
| Comparative Examples 1 | 13.4 |
| Comparative Examples 2 | 16.6 |
With reference to table 3, to compare with the 2 scouring make-up compositions that obtain with Comparative Examples 1, bracken spore powder itself is cleaned make-up composition with the cleansing cream that contains this bracken spore and is had the more excellent cuticular effect of removing.
Although containing Semen Armeniacae Amarum, the cosmetic composition for scrubbing that Comparative Examples 1 obtains cleans powder as abrasive cleaner, and has the excellent relatively cuticular effect of removing, but their skin of experimental subject complaint is upset, and in some experimental subjecies, erythrosis before sample treatment.Infer that skin irritation is owing to Semen Armeniacae Amarum scrub particle point causes firmly.
The sample that contains bracken spore that embodiment 1-6 obtains is chafe and being coated on the skin safely hardly.Inferring owing to the bracken spore smooth surface and because of physical force is broken hydranth makes sample not stimulate and safety.Under the situation of the sample that obtains for embodiment 4-6, bracken spore for binding agent with the bracken spore pearl that obtains bonded to each other, these pearls are also broken easily because of the physical force that applies of friction on skin, so bracken spore rubs on skin and do not have skin irritation.
Therefore, although conventional cosmetic composition for scrubbing only can use once weekly owing to chafe, cosmetic composition for scrubbing of the present invention is nonexpondable almost not to be had to stimulate and the effect of removing destratum corneum and washing one's face uniformly can be provided yet.
Industrial applicibility
As mentioned above, bracken spore has in its surface tiny hydranth and therefore has smooth surface, and be subject to physical friction power and can break easily. Therefore, the bracken spore that contains of the present invention is as the cosmetic composition for scrubbing of scrub particle chafe and have good use sensation and even and excellent scrub effect not. The bracken spore itself of collecting from wild pteridophyte can be used as scrub particle and joins and clean the make-up composition. If necessary, bracken spore can be bonded to each other with a plurality of bracken spores with adhesive and the form of the pearl that obtains adds. In this case, can control scouring intensity. And, when when each pearl forms coating, can improve the stability of these pearls in make-up composition and use sensation.
Claims (8)
1, a kind of cosmetic composition for scrubbing, said composition contain that to increase skin blood by friction on skin mobile and remove cuticular scrub particle, and wherein, this scrub particle is a bracken spore, and the mean diameter of described bracken spore is the 10-200 micron.
2, cosmetic composition for scrubbing as claimed in claim 1 wherein, is a benchmark with this scouring make-up composition, and the concentration of described bracken spore is 0.2-20 weight %.
3, cosmetic composition for scrubbing as claimed in claim 1, wherein, described bracken spore adds with the form of a plurality of bracken spores through binding agent pearl bonded to one another.
4, cosmetic composition for scrubbing as claimed in claim 3, wherein, described binding agent comprises and is selected from least a in the group of being made up of alginic acid, alginate, Polyethylene Glycol, polyvinyl pyrrolidone, polyvinyl alcohol, hydroxypropyl cellulose, methylcellulose, hydroxy methocel, hydroxypropyl emthylcellulose, carbopol, carboxymethyl cellulose, gelatin and starch.
5, cosmetic composition for scrubbing as claimed in claim 3, wherein, the mean diameter of described pearl is the 0.1-10 millimeter.
6, cosmetic composition for scrubbing as claimed in claim 3 wherein, also is formed with coating on the surface of each pearl.
7, cosmetic composition for scrubbing as claimed in claim 6, wherein, this coating is made by at least a material that is selected from the group of being made up of Polyethylene Glycol, polyvinyl pyrrolidone, hydroxypropyl cellulose, methylcellulose, hydroxy methocel, hydroxypropyl emthylcellulose, carbopol, gelatin, starch, Lac and SB.
8, cosmetic composition for scrubbing as claimed in claim 1, said composition are made into to be selected from the preparation in the group of being made up of cleansing cream, gel, foam, powder, body wash, scouring shampoo and massage cream.
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| Application Number | Priority Date | Filing Date | Title |
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| KR20040013797 | 2004-02-28 | ||
| KR1020040013797 | 2004-02-28 |
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| CN1921828A CN1921828A (en) | 2007-02-28 |
| CN100574745C true CN100574745C (en) | 2009-12-30 |
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| KR (1) | KR100614370B1 (en) |
| CN (1) | CN100574745C (en) |
| WO (1) | WO2005082328A1 (en) |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR100872481B1 (en) * | 2007-07-23 | 2008-12-05 | 정영모 | A lubricating composition with improved moisturizing property and anti-bacterial property |
| KR101350843B1 (en) * | 2011-09-05 | 2014-01-14 | 주식회사 제닉 | Cosmetic Composition for Scrubbing |
| KR102008060B1 (en) * | 2017-09-05 | 2019-10-21 | (주)프랜드 | Manufacture method of starch antibiosis scrub beads |
| KR20200040040A (en) | 2018-10-08 | 2020-04-17 | 수호세 주식회사 | Cosmetic composition for scrub cleansing |
| KR102215797B1 (en) * | 2019-06-28 | 2021-02-17 | 주식회사 비에프씨씨 | Method of manufacturing cosmetic composition including strawberry fruit |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR0163836B1 (en) * | 1995-12-29 | 1998-12-01 | Pacific Co Ltd | Cosmetic compositions containing scrub agents |
| US6495126B1 (en) * | 1999-07-20 | 2002-12-17 | Mary Kay Inc. | Treatment and composition for achieving skin anti-aging benefits by corneum protease activation |
| KR20030017300A (en) * | 2002-01-31 | 2003-03-03 | 주식회사 나우코스 | Cosmetic compositions containing extracts of Prunus armeniaca L, Vitis vinifera L. and Perilla frutescens var. japonica Hara |
| KR101008703B1 (en) * | 2003-11-17 | 2011-01-19 | 하병조 | Skin peeling cosmetic composition |
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2005
- 2005-02-28 CN CN200580005586A patent/CN100574745C/en active Active
- 2005-02-28 WO PCT/KR2005/000564 patent/WO2005082328A1/en active Application Filing
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| KR100614370B1 (en) | 2006-08-21 |
| CN1921828A (en) | 2007-02-28 |
| WO2005082328A1 (en) | 2005-09-09 |
| KR20060043290A (en) | 2006-05-15 |
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