CN104173208A - Dimming makeup base and preparation method thereof - Google Patents
Dimming makeup base and preparation method thereof Download PDFInfo
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- CN104173208A CN104173208A CN201410432206.1A CN201410432206A CN104173208A CN 104173208 A CN104173208 A CN 104173208A CN 201410432206 A CN201410432206 A CN 201410432206A CN 104173208 A CN104173208 A CN 104173208A
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- polydimethylsiloxane
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- light modulation
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- sun screen
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Abstract
The invention provides a dimming makeup base which comprises propylene glycol, glycerol, cyclopentasiloxane, octyl methoxycinnamate, tocopheryl acetate, synthetic grease, hectorite gel, nano-grade silicon treated titanium dioxide, polydimethylsiloxane, PEG-9 polydimethyl silica dimethylpolysiloxane, PEG-10 dimethyl polysiloxane, a mixture of dimethyl polysiloxane PEG-10/15 cross-linking polymer and dimethyl polysiloxane, phenyl trimethicone, polymethyl methacrylate, organic silicone elastomer, sodium citrate, sodium chloride, sodium hyaluronate, organic toner, preservative, silicon treatment pearl powder and the like. The dimming makeup base provided by the invention can effectively block makeup, has good effects of sun blocking, whitening and beautifying (physically) and moisturizing, can remarkably improve the stability, and meanwhile can effectively brighten the skin color and enable the skin to be in a natural glossy state.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of light modulation sun screen, and the preparation method of this light modulation sun screen.
Background technology
Sun screen is the cosmetics for the protection of skin, can isolate ultraviolet, and radioprotective contains Orangic sunscreen or physical sunscreen agent conventionally, and in addition, sun screen also has the effect of isolation color make-up, dust.
But, although at present commercially available sun screen generally all possesses effect of moisturizing, sun-proof, whitening (physics), isolation, but for bright color, improve skin dimness, matt aspect is not improved, and easily occurs the problems such as thinning, fuel-displaced, pigment is separated out.
Summary of the invention
An object of the present invention is the technical problem that will solve for above, provide one to there is the light modulation sun screen of moisturizing, sun-proof, whitening (physics), isolation color make-up and bright color effect.
Another object of the present invention is to provide the preparation method of described light modulation sun screen.
For reaching above object, the invention provides a kind of light modulation sun screen, its component by following percentage by weight forms: propylene glycol 5～7%, glycerol 5～7%, encircle five polydimethylsiloxane 6～10%, octyl methoxycinnamate 4～6%, tocopherol acetas 0.2～0.8%, synthetic ester oil 3～6%, Strese Hofmann's hectorite. gel 3～5%, nano silicone is processed titanium dioxide 2～4%, polydimethylsiloxane 2～4%, KF-6028 1.5～3.5%, KF6017 0.5～1%, the mixture 0.5～2% of KSG-210 and polydimethylsiloxane, phenyl gathers trimethicone 0.5～2%, polymethyl methacrylate 1～3%, elastomer silicone 2～5%, sodium citrate 0.2～0.5%, sodium chloride 0.5～0.8%, hyaluronate sodium 0.02～0.1%, inorganic toner 0.02～0.5%, antiseptic 0.2～0.5%, silicon is processed pearl essence 2～5%, water surplus.
Preferably, light modulation sun screen provided by the invention, is made up of the component of following percentage by weight:
Propylene glycol 5～6%, glycerol 6～7%, encircle five polydimethylsiloxane 8～10%, octyl methoxycinnamate 5～6%, tocopherol acetas 0.5～0.8%, synthetic ester oil 4.5～6%, Strese Hofmann's hectorite. gel 4～5%, nano silicone is processed titanium dioxide 3～4%, polydimethylsiloxane 2～3%, KF-6028 2.5～3.5%, KF6017 0.5～0.8%, the mixture 0.5～1% of KSG-210 and polydimethylsiloxane, phenyl gathers trimethicone 1.5～2%, polymethyl methacrylate 2～3%, elastomer silicone 3.5～5%, sodium citrate 0.2～0.35%, sodium chloride 0.5～0.8%, hyaluronate sodium 0.06～0.1%, inorganic toner 0.2～0.5%, antiseptic 0.2～0.3%, silicon is processed pearl essence 3.5～5%, water surplus.
Preferably, described synthetic ester oil be butanediol two sad/one or more mixture in dicaprate, propylene glycol dicaprylate/dicaprate, the different pelargonate of different tridecanol, glycerol three (thylhexoic acid) ester.
The mixture of one or more in BENTONE GEL VS-5PC V, BENTONE GEL ISD V, BENTONE GEL MIO V that preferably, described Strese Hofmann's hectorite. gel is ELEMENTIS.
Preferably, described elastomer silicone be Shin Etsu company KSG-16, KSG-19, KSG-016F or Dow Corning company 9045, one or more mixture in FB-9586.
The mixture of one or more in titanium dioxide that preferably, described inorganic toner is triethoxy octyl group siloxane treated, iron oxide red, iron oxide yellow, iron oxide black, manganese violet, chrome oxide green, ultramarine blue.
Preferably, in the mixture of described KSG-210 and polydimethylsiloxane, the content of described KSG-210 is 20～30wt%, and the content of polydimethylsiloxane is 70～80wt%.
The present invention also provides the preparation method of above-mentioned light modulation sun screen, and its step is as follows:
1. hyaluronate sodium and antiseptic are joined in propylene glycol, glycerol and be uniformly dispersed, then add sodium citrate, sodium chloride and water, be stirred to transparent solution, stand-by;
2. synthetic ester oil, nano silicone are processed after titanium dioxide and inorganic toner mixing and stirring, ground twice with three-roller or colloid mill and be uniformly dispersed to pigment, add emulsifying pot;
3. ring five polydimethylsiloxane, octyl methoxycinnamate, tocopherol acetas, Strese Hofmann's hectorite. gel, polydimethylsiloxane, KF-6028, KF6017, KSG-210 and polydimethylsiloxane, the poly-trimethicone of phenyl, polymethyl methacrylate, elastomer silicone are added to emulsifying pot successively, stir homogenizing;
4. slowly add while stirring the material of step 1 to emulsifying pot, homogenizing after stirring;
5. under stirring, slowly add silicon to process pearl essence, stir, then discharging.
Compared with prior art, light modulation sun screen of the present invention can effectively be isolated color make-up, has good sun-proof, whitening (physics), moisture-keeping efficacy, and can significantly improve the stability of sun screen, simultaneously effective bright color, allows skin reach the state of natural gloss.
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme of the present invention is described in further detail, but protection scope of the present invention is not limited in following examples.The cited component raw material of the embodiment of the present invention is existing, can buy by commercial channel.For example, silicon is processed pearl essence purchased from SENSIENT company, KOBO company, DAITO company etc.; To be that this area is conventional meet safety criterion to described synthetic ester oil, can be butanediol two sad/one or more mixture in dicaprate, propylene glycol dicaprylate/dicaprate, the different pelargonate of different tridecanol, glycerol three (thylhexoic acid) ester; The mixture of one or more in BENTONE GEL VS-5PC V, BENTONE GEL ISD V, BENTONE GEL MIO V that described Strese Hofmann's hectorite. gel can be ELEMENTIS; Described elastomer silicone can be Shin Etsu company KSG-16, KSG-19, KSG-016F or Dow Corning company 9045, one or more mixture in FB-9586; The mixture of one or more in titanium dioxide that described inorganic toner can be triethoxy octyl group siloxane treated, iron oxide red, iron oxide yellow, iron oxide black, manganese violet, chrome oxide green, ultramarine blue.In the mixture of described KSG-210 and polydimethylsiloxane, the content of described KSG-210 is 20～30wt%, the content of polydimethylsiloxane is 70～80wt%, for example the KSG-210 of Shin Etsu company.
Weigh the each component of light modulation sun screen of embodiment 1～3 according to following table:
Light modulation sun screen according to following steps Preparation Example 1～3:
1. hyaluronate sodium and antiseptic are joined in propylene glycol, glycerol and be uniformly dispersed, then add sodium citrate, sodium chloride and water, be stirred to transparent solution, stand-by;
2. synthetic ester oil, nano silicone are processed after titanium dioxide and inorganic toner mixing and stirring, ground twice with three-roller or colloid mill and be uniformly dispersed to pigment, add emulsifying pot;
3. ring five polydimethylsiloxane, octyl methoxycinnamate, tocopherol acetas, Strese Hofmann's hectorite. gel, polydimethylsiloxane, KF-6028, KF6017, KSG-210 and polydimethylsiloxane, the poly-trimethicone of phenyl, polymethyl methacrylate, elastomer silicone are added to emulsifying pot successively, stir homogenizing;
4. slowly add while stirring the material of step 1 to emulsifying pot, homogenizing after stirring;
5. under stirring, slowly add silicon to process pearl essence, stir, then discharging.
The performance of the moisturizing of the light modulation sun screen of the test embodiment of the present invention 1～3, sun-proof, whitening (physics), stability, bright color.
1. high low temperature stability test
The sun screen of preparation is packed in the PET bottle of 30ML, be placed in respectively the stability under its heat-resisting, cold-resistant and room temperature of constant temperature test box (refrigerator or biochemical cultivation case) test of 48 DEG C, 40 DEG C ,-18 DEG C, 25 DEG C, in the time of 24 hours, 1 week, 2 weeks, 4 weeks, 8 weeks and 12 weeks, (returning to room temperature) observes product respectively, judges according to following 4 grade determinating references.
Before A and test, outward appearance no significant difference, without oil-water separation phenomenon, without coarse or without other ANOMALOUS VARIATIONS;
Before B and test, slightly change;
Before C and test, medium variation;
Before D and test, significant change.
(remarks: change and refer to oil-water separation, coarse, there is the wild effects such as pigment figure, can be that wherein one or more phenomenons occur simultaneously.)
2, improve the evaluation test of the good degree of gloss
Subjects: 30 routine women, 34.5 ± 11.5 years old mean age.The light modulation sun screen of smearing respectively embodiment 1～3 in the present invention at left face and right face, tester sits quietly after 30min, carries out the scoring of 5 grades according to following evaluation, calculates its meansigma methods by all overall scores.
4 points: very good
3 points: good
2 points: general
1 point: poor
0 point: non-constant
| Test effect | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| High low-temperature stability | A | B | A |
| Glossiness is evaluated | 2.900 | 3.467 | 3.233 |
| Performance of keeping humidity | Well | Well | Well |
| Sun-proof performance | Well | Well | Well |
| Whitening (physics) performance | Well | Well | Well |
According to test result, visible, the light modulation sun screen stable performance of the embodiment of the present invention 1～3, obviously can improve the glossiness of skin better, and possesses good moisture-keeping efficacy, sun-proof function and whitening (physics) effect.
Claims (8)
1. a light modulation sun screen, it is characterized in that being formed by the component of following percentage by weight: propylene glycol 5～7%, glycerol 5～7%, encircle five polydimethylsiloxane 6～10%, octyl methoxycinnamate 4～6%, tocopherol acetas 0.2～0.8%, synthetic ester oil 3～6%, Strese Hofmann's hectorite. gel 3～5%, nano silicone is processed titanium dioxide 2～4%, polydimethylsiloxane 2～4%, KF-6028 1.5～3.5%, KF6017 0.5～1%, the mixture 0.5～2% of KSG-210 and polydimethylsiloxane, phenyl gathers trimethicone 0.5～2%, polymethyl methacrylate 1～3%, elastomer silicone 2～5%, sodium citrate 0.2～0.5%, sodium chloride 0.5～0.8%, hyaluronate sodium 0.02～0.1%, inorganic toner 0.02～0.5%, antiseptic 0.2～0.5%, silicon is processed pearl essence 2～5%, water surplus.
2. light modulation sun screen according to claim 1, it is characterized in that being formed by the component of following percentage by weight: propylene glycol 5～6%, glycerol 6～7%, encircle five polydimethylsiloxane 8～10%, octyl methoxycinnamate 5～6%, tocopherol acetas 0.5～0.8%, synthetic ester oil 4.5～6%, Strese Hofmann's hectorite. gel 4～5%, nano silicone is processed titanium dioxide 3～4%, polydimethylsiloxane 2～3%, KF-6028 2.5～3.5%, KF6017 0.5～0.8%, the mixture 0.5～1% of KSG-210 and polydimethylsiloxane, phenyl gathers trimethicone 1.5～2%, polymethyl methacrylate 2～3%, elastomer silicone 3.5～5%, sodium citrate 0.2～0.35%, sodium chloride 0.5～0.8%, hyaluronate sodium 0.06～0.1%, inorganic toner 0.2～0.5%, antiseptic 0.2～0.3%, silicon is processed pearl essence 3.5～5%, water surplus.
3. light modulation sun screen according to claim 1 and 2, is characterized in that: described synthetic ester oil be butanediol two sad/one or more mixture in dicaprate, propylene glycol dicaprylate/dicaprate, the different pelargonate of different tridecanol, glycerol three (thylhexoic acid) ester.
4. light modulation sun screen according to claim 1 and 2, is characterized in that: the mixture of one or more in BENTONE GEL VS-5PC V, BENTONE GEL ISD V, BENTONE GEL MIO V that described Strese Hofmann's hectorite. gel is ELEMENTIS.
5. light modulation sun screen according to claim 1 and 2, is characterized in that: described elastomer silicone be Shin Etsu company KSG-16, KSG-19, KSG-016F or Dow Corning company 9045, one or more mixture in FB-9586.
6. light modulation sun screen according to claim 1 and 2, is characterized in that: the mixture of one or more in titanium dioxide that described inorganic toner is triethoxy octyl group siloxane treated, iron oxide red, iron oxide yellow, iron oxide black, manganese violet, chrome oxide green, ultramarine blue.
7. light modulation sun screen according to claim 1 and 2, it is characterized in that: in the mixture of described KSG-210 and polydimethylsiloxane, the content of described KSG-210 is 20～30wt%, and the content of polydimethylsiloxane is 70～80wt%.
8. the preparation method of the light modulation sun screen described in claim 1 to 7 any one, its step is as follows:
(1) hyaluronate sodium and antiseptic are joined in propylene glycol, glycerol and be uniformly dispersed, then add sodium citrate, sodium chloride and water, be stirred to transparent solution, stand-by;
(2) synthetic ester oil, nano silicone are processed after titanium dioxide and inorganic toner mixing and stirring, ground twice and be uniformly dispersed to pigment, add emulsifying pot;
(3) ring five polydimethylsiloxane, octyl methoxycinnamate, tocopherol acetas, Strese Hofmann's hectorite. gel, polydimethylsiloxane, KF-6028, KF6017, KSG-210 and polydimethylsiloxane, the poly-trimethicone of phenyl, polymethyl methacrylate, elastomer silicone are added to emulsifying pot successively, stir homogenizing;
(4) slowly add while stirring the material of step 1 to emulsifying pot, homogenizing after stirring;
(5) under stirring, slowly add silicon to process pearl essence, stir, then discharging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410432206.1A CN104173208B (en) | 2014-08-28 | 2014-08-28 | Dimming makeup base and preparation method thereof |
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| CN201410432206.1A CN104173208B (en) | 2014-08-28 | 2014-08-28 | Dimming makeup base and preparation method thereof |
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| CN104173208A true CN104173208A (en) | 2014-12-03 |
| CN104173208B CN104173208B (en) | 2017-05-24 |
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Cited By (5)
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| CN104586648A (en) * | 2014-12-26 | 2015-05-06 | 广州神采化妆品有限公司 | Intelligent color mixing BB cream and preparation method thereof |
| CN107536718A (en) * | 2017-09-29 | 2018-01-05 | 广东馨柯生命科学有限公司 | A kind of long-acting slow-release whitening snow defrosting and preparation method thereof |
| CN104546553B (en) * | 2014-12-19 | 2018-04-20 | 广州神采化妆品有限公司 | Pore stealth cream base and preparation method thereof |
| CN109640941A (en) * | 2016-06-13 | 2019-04-16 | 株式会社爱茉莉太平洋 | Odorlessness and highly stable cosmetic composition |
| CN112603838A (en) * | 2020-11-30 | 2021-04-06 | 上海蔻沣生物科技有限公司 | Nano titanium dioxide slurry oil and preparation method and application thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104546553B (en) * | 2014-12-19 | 2018-04-20 | 广州神采化妆品有限公司 | Pore stealth cream base and preparation method thereof |
| CN104586648A (en) * | 2014-12-26 | 2015-05-06 | 广州神采化妆品有限公司 | Intelligent color mixing BB cream and preparation method thereof |
| CN104586648B (en) * | 2014-12-26 | 2017-10-31 | 广州神采化妆品有限公司 | A kind of intelligence toning BB frosts and preparation method thereof |
| CN109640941A (en) * | 2016-06-13 | 2019-04-16 | 株式会社爱茉莉太平洋 | Odorlessness and highly stable cosmetic composition |
| CN109640941B (en) * | 2016-06-13 | 2022-04-22 | 株式会社爱茉莉太平洋 | Odorless and highly stable cosmetic composition |
| CN107536718A (en) * | 2017-09-29 | 2018-01-05 | 广东馨柯生命科学有限公司 | A kind of long-acting slow-release whitening snow defrosting and preparation method thereof |
| CN112603838A (en) * | 2020-11-30 | 2021-04-06 | 上海蔻沣生物科技有限公司 | Nano titanium dioxide slurry oil and preparation method and application thereof |
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