WO1997031615A1 - Dispositif pressurise transparent a composition moussante comprenant des tensioactifs non-ioniques et amphoteres - Google Patents
Dispositif pressurise transparent a composition moussante comprenant des tensioactifs non-ioniques et amphoteres Download PDFInfo
- Publication number
- WO1997031615A1 WO1997031615A1 PCT/FR1997/000206 FR9700206W WO9731615A1 WO 1997031615 A1 WO1997031615 A1 WO 1997031615A1 FR 9700206 W FR9700206 W FR 9700206W WO 9731615 A1 WO9731615 A1 WO 9731615A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- oxyethylenated
- mono
- stearate
- polyethylene glycol
- surfactant
- Prior art date
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4993—Derivatives containing from 2 to 10 oxyalkylene groups
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/26—Optical properties
- A61K2800/262—Transparent; Translucent
Definitions
- the subject of the invention is new pressurized devices comprising a composition, in particular a cosmetic or dermatological composition, and in particular a cleaning and make-up removing composition.
- Cleansing the skin is very important for facial care. It must be as efficient as possible because fatty residues such as excess sebum, the remains of cosmetic products used daily, in particular make-up products, and in particular water-resistant "waterproof” products, accumulate in the skin folds and can clog the pores of the skin and lead to the appearance of pimples.
- the usual makeup removers are usually in the form of a gel, lotion or cream. However, the market awaits new forms of products, both more aesthetic and possibly fun. To meet this expectation, new make-up removers and cleansers for the skin have appeared, in the form of transparent pressurized devices, containing a cleansing and make-up remover composition which is transparent, monophasic and foaming.
- compositions for topical application packaged in pressurized, foaming, transparent, single-phase and stable bottles.
- These compositions comprise a surfactant and a propellant gas in an aqueous-alcoholic medium.
- the alcohol is preferably a C ⁇ Ca monohydric alcohol.
- Document EP-676188 discloses a similar device, comprising a monophasic, fluid composition, free of monohydric alcohol, consisting of a propellant gas and an aqueous concentrate.
- the propellant comprises a mixture of dimethyl ether and hydrocarbon gas; the aqueous concentrate comprises surfactants and further a coupling agent.
- dimethyl ether is a flammable gas with a very low flash point. Its use therefore increases the risks associated with pressurized devices, both for the production site and for the user of this device.
- Canadian patent CA-1002256 discloses a transparent, uniform pressurized system usable for the distribution of transparent aqueous cosmetic products, including makeup-removing products.
- the use as a surfactant of a triethanolamine salt of an acyl lactylic acid makes it possible to obtain a system in which the propellant gas is completely dissolved in the aqueous phase.
- a transparent pressurized system comprising a foaming transparent composition, free from alcohol.
- This composition comprises an aqueous solution of a foaming surfactant, which is generally anionic, in which a liquid propellant is dispersed by means of a second surfactant, soluble in the propellant and insoluble in water.
- compositions described in all of these documents and used for cleaning the skin essentially consist of anionic surfactants, which destroy the hydro-lipid film of the skin and leave the skin clean but rough.
- the subject of the invention is a pressurized device comprising
- composition B comprises a mixture of surfactants chosen from nonionic surfactants and amphoteric surfactants.
- compositions of the invention are dispensed in the form of a creamy foam which cleanses the skin without attacking it.
- the absence of anionic and cationic surfactants in the compositions distributed by this device has the effect of obtaining a foam of a product which is extremely gentle for the skin and for the mucous membranes (lips, inside of the eyelids), which allows its use for cleansing and removing makeup from the face, in particular removing makeup from the eyes.
- the pressurized bottles used in the invention are transparent.
- Such bottles are well known to those skilled in the art and in common use, one can for example refer to patent application WO95 / 05796 on the subject of these bottles. They particularly highlight the surprising character of the invention: through the bottle, a transparent emulsion is observed, having a fluidity comparable to that of water, said emulsion being restored in the form of a smooth foam through the means of distribution, and not in the form of a spray as expected a priori.
- Any means of dispensing an aerosol can known to those skilled in the art can be used.
- a bottle and a dispensing means which can be used in the present invention is for example shown in patent application FR-95-12788.
- transparent means that through the bottle containing the composition one can distinguish the characters printed on a newspaper page placed behind this bottle. This term also means that a 10cm thick sample of the composition has a maximum light transmission of at least 4% in any wavelength between 200nm and 800nm.
- the subject of the invention is a pressurized device as described above, characterized in that the aqueous composition B comprises:
- the aqueous composition B comprises 1 to 25% by weight of at least one nonionic emulsifying surfactant.
- the aqueous composition B comprises 1 to 30% of at least one nonionic thickening surfactant.
- the composition of B is adjusted, and in particular the choice and the percentage of the thickener (s), so that this composition B has a Brookfield viscosity of between 5 and 200mPa.s, and preferably between 10 and 150mPa. s.
- propellants known for such applications. Mention may in particular be made of hydrocarbon gases, such as, for example, propane, n-butane, isobutane and their mixtures; fluorinated gases such as, for example, chlorodifluoro methane, dichlorodifluoromethane, difluoroethane, chlorodifluoroethane, dichlorotetrafluoroethane etc. and their mixtures; nitrogen, air and carbon dioxide and mixtures thereof can also be used as propellants in the present invention.
- hydrocarbon gases having from 2 to 6 carbon atoms.
- those having from 1.5 to 4%, by weight relative to the total weight of the composition, of propellant gas are preferred.
- the emulsifying surfactants which can be used in the present invention are preferably chosen from those having an HLB balance of between
- HLB balance hydrophilic-lipophilic balance
- L represents the percentage by weight of the lipophilic group relative to the weight of the whole molecule.
- these surfactants are chosen from the products of addition of 1 to 200 moles of ethylene oxide or of propylene oxide on partial esters of polyols having 2 to 16 carbon atoms and of fatty acids having 12 to 22 carbon atoms.
- products such as described above are chosen having an esterification rate less than or equal to 2.
- the nonionic thickening surfactants which can be used in the present invention are preferably chosen from: ⁇ - C r C 6 alkanolamides of C 8 -C 22 alkyl ether carboxylic acids; ⁇ - the adducts of 10 to 300 moles of ethylene oxide or propylene oxide on partial esters of polyols having 2 to 16 carbon atoms and of fatty acids having 12 to 22 carbon atoms.
- esterification rate greater than or equal to 2; ⁇ - C 12 -C 22 fatty alcohols polyoxyethylenated and / or polyoxypropylenated and / or polyglycerolated, ⁇ - C 12 -C 22 fatty esters of polyoxyethylene and / or polyoxypropylene and / or polyglycerol, ⁇ - block polymers polyethylene glycol and / or polypropylene glycol.
- compositions according to the invention comprise at least two thickening surfactants each belonging to two different families, among the families of thickeners ⁇ to ⁇ described above.
- C r C ⁇ alkanolamide of C 8 -C 22 alkyl ether carboxylic acid denotes products corresponding to formula I:
- R can be chosen from stearyl, oleyl, ricinoleyl, linoleyl, lauryl, myristyle, capryle, palmityl radicals or from mixtures of C 8 -C 22 alkyl radicals.
- R 'can for example be chosen from methyl, ethyl, n-propyl, isopropyl, terbutyl and n-hexyl radicals.
- partial polyol esters which can be used in the present invention, mention may be made in particular of those derived from glycol, glycerol and sugars, such as, for example, glucose, fructose, maltose, ribose, arabinose, xylose, lyxose, ribulose, xylulose, allose, altrose, mannose, gulose, galactose, sucrose, sorbitol.
- sugars such as, for example, glucose, fructose, maltose, ribose, arabinose, xylose, lyxose, ribulose, xylulose, allose, altrose, mannose, gulose, galactose, sucrose, sorbitol.
- thickening surfactants which can be used in the present invention, there may be mentioned, for example, the following products: castor oil, monoethanol-alkyl acid amides (C 13 , C 15 ) carboxylic ether (2 EO), monoethanolamide carboxylic ether acid (50 EO), oxyethylenated tallow mono- and di-glycerides (200 EO), oxyethylenated tallow mono- and di-glycerides (82 EO), oxyethylenated coconut mono- and di-glycerides (78 EO), triglycerides of stearic and hydroxystearic acid (40 EO), polyethylene glycol mono-stearate (100 EO), polyglycerolated alcohol dodecanediol (3.5 mo!
- the C r C 6 alkanolamides of C 8 -C 22 alkyl ether carboxylic acids are for example marketed by the company HENKEL under the brand COMPERLAN, or by the company CHEM Y under the brand name AMINOL;
- the products of addition of ethylene oxide or of propylene oxide to partial esters of polyols and of fatty acids are, for example, marketed by the company BASF under the brand CREMOPHOR, or by the company AMERCHOL under the brand GLUCAMATE;
- polyoxyethylenated and / or polyoxypropylenated and / or polyglycerolated C 12 -C 22 fatty alcohols are for example sold by the company ICI under the brand BRU,
- the C 12 -C 22 fatty esters of polyoxyethylene and / or of polyoxypropylene and / or of polyglycerol are, for example, sold by the company ICI under the brand MYRJ,
- the block polymers of polyethylene glycol and / or of polypropylene glycol are for example marketed by the company ICI under the brand SYNPERONIC.
- the invention relates to a pressurized device as described above, characterized in that the aqueous composition B comprises:
- compositions of the present invention preferably comprise from 3 to 10% of at least one thickening surfactant as defined above.
- the amount of thickener used is adapted to satisfy the viscosity criterion given above. An excessive amount of this type of compound can cause significant thickening of the composition of the invention, which then becomes difficult to distribute as an aerosol. Too small a quantity has the disadvantage of jeopardizing the stability of the composition.
- compositions B also comprise at least one alkylpolyglucoside as non-ionic surfactant.
- this alkylpolyglucoside represents from 0.01 to 10% by weight of B.
- the aqueous composition B also comprises at least one amphoteric surfactant, advantageously in amounts ranging from 0.01 to 15% by weight of B and even more preferably from 1 to 5% by weight of B.
- B comprises:
- compositions B can comprise up to about 98% water.
- water is understood to mean pure demineralized water.
- all or part of the water used in compositions B can optionally be chosen from mineral or thermal waters.
- mineral water is fit for consumption, which is not always the case with thermal water.
- Each of these waters contains, among other things, dissolved minerals and trace elements. These waters are known to be used for specific treatment purposes according to the specific trace elements and minerals they contain, such as hydration and desensitization of the skin or the treatment of certain dermatoses.
- mineral or thermal water we will not only denote natural mineral or thermal water, but also natural mineral or thermal water enriched with mineral constituents and / or additional trace elements, as well as aqueous mineral and / or trace element solutions prepared from purified water (demineralized or distilled).
- a natural thermal or mineral water used according to the invention can, for example, be chosen from Vittel water, water from the Vichy basin, water from Uriage, water from La Roche Posay, water from Bourboule, water from Enghien-les-Bains, water from Saint Gervais-les-Bains, water from Néris-les-Bains, water from Allevar-les-Bains, water from Digne, Maizines water, Neyrac-les- Bains water, Lons-le-Saunier water, Eaux Bonnes, Rochefort water, Saint Christau water, Fumades water and the water of Tercis-les-Bains, the water of Avene.
- compositions of the invention can, in addition, contain adjuvants customary in the fields concerned such as preservatives, antioxidants, perfumes, filters, coloring matters, hydrophilic or lipophilic active agents.
- the active ingredients for the skin can be anti-aging active agents, anti-wrinkle active agents, moisturizers or humectants, depigmenting active agents, anti-free radical active agents (radical oxygen species), nutritive active agents, active protective, restructuring active, firming active, anti-acne active, exfoliating active, emollient active or active treating skin diseases such as yeast, dermatitis, psoriasis, etc.
- active agents are used, depending on their nature, in the usual proportions and for example from 0.01% to 10% by weight relative to the total weight of the composition.
- anti-acne anti-aging, anti-wrinkle, moisturizing, exfoliating active agents
- ⁇ -hydroxy acids glycolic, lactic, malic, citric acids, etc.
- antioxidants examples include sulfites.
- compositions named B, to B 1 ⁇ were prepared in accordance with the information given in table I. These compositions are then introduced into a pressurized bottle fitted with a dispensing head into which a pressurized gas is introduced. The whole is stirred so as to obtain a homogeneous mixture of the two initial phases.
- the devices are evaluated in Table I.
- amphoteric surfactant N-cocoyl amidoethyl, N-ethoxycarboxymethyl sodium glycinate is marketed under the name of "Miranol C2M” by the company Rhône-Poulenc, the “Plantaren 2000", marketed by the company Henkel, is a mixture of alkyl (C Intel/ C 10 / C 12 / C 14 / C 1 ⁇ 29/37/23/9/2) polyglucosides,“ TWEEN 20 ”denotes oxyethylenated sorbitan mono-laurate (20 OE) (nonionic surfactant) marketed by ICI. With the exception of Lucas water, the water used in the examples is demineralized water.
- the viscosity of the aqueous compositions B was evaluated at B 1 ⁇ in mPa.s, then these aqueous compositions were conditioned in transparent pressurized bottles by introducing into these bottles 97% by weight of the composition and 3% by weight of isobutane . We then measured the transparency and stability, after several months of storage at room temperature, of these pressurized devices. The viscosity is given in mPa.s. It is measured at 25 ° C. using a Brookfield viscometer, the speed of the rotating module (module I) being fixed at 5 revolutions / min. transparency is noted +, 0, or -:
- the different thickeners are designated E 1 to E 10 :
- E 4 stearic acid amide (C 16 / C 18. 30/70) (50 EO)
- E 5 methyl glucoside di-oleate (120 EO)
- E 10 oxyethylenated palm glyceride (200 EO) and oxyethylenated coconut glyceride (70 EO) (80/20)
- compositions with the exception of B 3 are transparent and do not exhibit a halo, both at the time of their preparation and after several months of storage.
- Example B 3 is not part of the invention.
Abstract
Description
Claims
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
BR9702102A BR9702102A (pt) | 1996-03-01 | 1997-02-03 | Dispositivo pressurizado |
JP9530660A JP2988730B2 (ja) | 1996-03-01 | 1997-02-03 | 非イオン性および両性の界面活性剤を含有する起泡性組成物用の透明な加圧装置 |
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR96/02628 | 1996-03-01 | ||
FR9602628A FR2745496B1 (fr) | 1996-03-01 | 1996-03-01 | Dispositif pressurise transparent a composition moussante comprenant des tensioactifs non-ioniques et amphoteres |
CN97190124A CN1082802C (zh) | 1996-03-01 | 1997-02-03 | 用于含非离子和两性表面活性剂的起泡组合物的透明增压装置 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO1997031615A1 true WO1997031615A1 (fr) | 1997-09-04 |
Family
ID=25744436
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/FR1997/000206 WO1997031615A1 (fr) | 1996-03-01 | 1997-02-03 | Dispositif pressurise transparent a composition moussante comprenant des tensioactifs non-ioniques et amphoteres |
Country Status (13)
Country | Link |
---|---|
US (1) | US5888478A (fr) |
EP (1) | EP0792632B2 (fr) |
JP (1) | JP2988730B2 (fr) |
CN (1) | CN1082802C (fr) |
AT (1) | ATE165731T1 (fr) |
BR (1) | BR9702102A (fr) |
CA (1) | CA2217289A1 (fr) |
DE (1) | DE69700006T3 (fr) |
ES (1) | ES2116818T3 (fr) |
FR (1) | FR2745496B1 (fr) |
PL (1) | PL323179A1 (fr) |
RU (1) | RU2152782C2 (fr) |
WO (1) | WO1997031615A1 (fr) |
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US6300508B1 (en) * | 1997-07-30 | 2001-10-09 | Henkel Kommanditgesellschaft Auf Aktien | Thickened aqueous surfactant solutions |
DE19753108A1 (de) † | 1997-11-29 | 1999-08-05 | Wella Ag | Mittel zur Erhöhung der Formbarkeit und des Glanzes von Haaren |
GB9810949D0 (en) * | 1998-05-22 | 1998-07-22 | Hewlett Healthcare Limited | Formulation |
US7074264B2 (en) * | 2000-03-31 | 2006-07-11 | Spuni Comércio de Produtos Esportivos E Marketing Ltda. | Foaming aqueous composition, use thereof and process for temporary demarcation of regulation distances in sports |
KR100763305B1 (ko) | 2000-03-31 | 2007-10-04 | 케미커 도 브라질 프로듀토스 오토모티보스 엘티디에이 | 발포성 수성 조성물, 그의 용도 및 스포츠에서 규정된거리의 경계를 일시적으로 설정하는 방법 |
JP2004503570A (ja) * | 2000-07-14 | 2004-02-05 | ジョンソン・アンド・ジョンソン・コンシューマー・カンパニーズ・インコーポレイテッド | 自己発泡性洗浄用ゲル |
JP3704605B2 (ja) * | 2001-06-27 | 2005-10-12 | 株式会社マンダム | 皮膚洗浄用シート |
DE10134597A1 (de) * | 2001-07-17 | 2003-02-06 | Beiersdorf Ag | Schäumbare Zubereitungen |
DE50204757D1 (de) * | 2001-09-25 | 2005-12-08 | Mibelle Ag Cosmetics Buchs | Nachschäumendes kosmetisches Gel und Verfahren zu dessen Herstellung |
US6915038B2 (en) * | 2002-09-13 | 2005-07-05 | The Boeing Company | Optical corner coupler system and method |
KR101052677B1 (ko) | 2004-04-20 | 2011-07-28 | (주)아모레퍼시픽 | 빠른 전상과 반투명한 외관을 갖는 마사지용 화장료 조성물 |
US7488709B2 (en) * | 2004-11-26 | 2009-02-10 | L'oreal S.A. | Cleansing composition in the form of an aerosol foam without anionic surfactant, and uses in cosmetics |
FR2878440B1 (fr) * | 2004-11-26 | 2008-05-30 | Oreal | Composition de nettoyage sous forme de mousse aerosol sans tensioactif anionique et utilisations en cosmetique |
JP4423237B2 (ja) * | 2005-06-13 | 2010-03-03 | 太陽化学株式会社 | 洗浄剤用増粘剤 |
DE102006020404A1 (de) * | 2006-05-03 | 2007-11-08 | Cognis Ip Management Gmbh | Verdickungsmittel |
US7723279B2 (en) | 2006-08-23 | 2010-05-25 | The Clorox Company | Foamable compositions containing alcohol |
US20100189809A1 (en) * | 2006-08-23 | 2010-07-29 | The Clorox Company | Foamable Compositions Containing Alcohol |
RU2732490C2 (ru) * | 2016-11-29 | 2020-09-17 | Акционерное общество "Международный инновационный нанотехнологический центр" | Композиция для футбольной исчезающей пены |
CN114446405A (zh) * | 2020-11-06 | 2022-05-06 | 四川大学 | 一种预测二氧化碳醇胺吸收剂分相行为的模型 |
FR3124704B1 (fr) * | 2021-06-30 | 2024-02-16 | Oreal | Composition d’apparence monophasique comprenant un tensioactif non ionique et un tensioactif amphotère |
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1996
- 1996-03-01 FR FR9602628A patent/FR2745496B1/fr not_active Expired - Lifetime
-
1997
- 1997-02-03 EP EP97400242A patent/EP0792632B2/fr not_active Expired - Lifetime
- 1997-02-03 AT AT97400242T patent/ATE165731T1/de not_active IP Right Cessation
- 1997-02-03 CN CN97190124A patent/CN1082802C/zh not_active Expired - Fee Related
- 1997-02-03 ES ES97400242T patent/ES2116818T3/es not_active Expired - Lifetime
- 1997-02-03 BR BR9702102A patent/BR9702102A/pt unknown
- 1997-02-03 PL PL97323179A patent/PL323179A1/xx unknown
- 1997-02-03 JP JP9530660A patent/JP2988730B2/ja not_active Expired - Fee Related
- 1997-02-03 RU RU97119623/14A patent/RU2152782C2/ru active
- 1997-02-03 CA CA002217289A patent/CA2217289A1/fr not_active Abandoned
- 1997-02-03 DE DE69700006T patent/DE69700006T3/de not_active Expired - Lifetime
- 1997-02-03 WO PCT/FR1997/000206 patent/WO1997031615A1/fr active IP Right Grant
- 1997-02-28 US US08/808,416 patent/US5888478A/en not_active Expired - Lifetime
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Also Published As
Publication number | Publication date |
---|---|
RU2152782C2 (ru) | 2000-07-20 |
FR2745496A1 (fr) | 1997-09-05 |
DE69700006D1 (de) | 1998-06-10 |
EP0792632A1 (fr) | 1997-09-03 |
US5888478A (en) | 1999-03-30 |
DE69700006T3 (de) | 2012-10-18 |
JP2988730B2 (ja) | 1999-12-13 |
CN1082802C (zh) | 2002-04-17 |
EP0792632B2 (fr) | 2011-02-16 |
EP0792632B1 (fr) | 1998-05-06 |
DE69700006T2 (de) | 1998-08-20 |
ATE165731T1 (de) | 1998-05-15 |
ES2116818T3 (es) | 1998-07-16 |
CN1180307A (zh) | 1998-04-29 |
FR2745496B1 (fr) | 1998-04-30 |
BR9702102A (pt) | 1999-07-20 |
CA2217289A1 (fr) | 1997-09-04 |
PL323179A1 (en) | 1998-03-16 |
JPH10506654A (ja) | 1998-06-30 |
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